Table 1.
Entry | Alcohol/amine | Yield (%) | Entry | Alcohol | Yield (%) |
---|---|---|---|---|---|
1 | 66 | 8 | 0 | ||
2 | 53 | 9 | 60 | ||
3 | 78 | 10 | b | ||
4 | 63 | 11 | 65 | ||
5 | 0 | 12 | 0 | ||
6 | 53 | 13 | 0 | ||
7 | 0 |
Reactions carried out using 1% catalyst and 4 equiv alcohol at room temperature for 24 h in CH2Cl2.
Unidentified product.