Table 1a.
Data collection | ||
---|---|---|
Mutant | Y54F(biotin complex) | Y54F(uncomplexed) |
Unit cell dimensions (a,b,c,) | 46.61, 94.11, 104.60 Å | 57.273, 57.273, 171.715 Å |
(α, β, γ) | 90., 90., 90. ° | 90., 90., 90. ° |
Space group | I222 | I4122 |
Resolution | 50.0-1.22 Å (1.26-1.22) | 36.6-1.15 Å (1.21-1.15) |
Unique reflections | 68448 | 51198 |
Completeness (last shell) | 99.8% (98.4%) | 99.1% (93.6%) |
Redundancy (last shell) | 13.4 (10.0) | 14.7 (9.6) |
I/sigma (last shell) | 23.1 (3.0) | 21.8 (2.3) |
Rmerge (last shell) | 0.121 (0.613) | 0.057 (0.967) |