Table 2.
Stability test conditions | Conc. (ng/ml) | % change | SD |
---|---|---|---|
Four freeze–thaw cycles, plasma | 120 | 1.4 | 7 |
170,000 | 1.2 | 1249 | |
| |||
RT (22–28°C), 3 days, plasma | 120 | 11.9 | 4 |
170,000 | −1.6 | 404 | |
| |||
RT (22°C), 72 h, autosampler | 120 | 4.7 | 3.0 |
170,000 | −3.3 | 814 | |
| |||
−70°C, 1 year, plasma | 120 | 10 | 5 |
170,000 | 7.0 | 796 | |
−70°C, 1.5 year stock in 0.5% FA, 50% MeCN | −0.53 | 0.1 |
FA: Formic acid; MeCN: Acetonitrile; RT: Room temperature.