TABLE 1.
Data collection statistics
Values in parentheses are for the highest-resolution shell.
| Non-glycosylated LeIBPSe-Met peak single-wavelength anomalous dispersion | Glycosylated LeIBP | |
|---|---|---|
| Data collection | ||
| Space group | P43212 | P6522 |
| Cell dimensions | ||
| a, b, c (Å) | 97.6, 97.6, 106.6 | 58.6, 58.6, 292.6 |
| α, β, γ (°) | 90.0, 90.0, 90.0 | 90.0, 90.0, 120.0 |
| Wavelength | 0.98227 | 1.54180 |
| Resolution (Å) | 35.99-1.57 (1.66-1.57) | 50.78-2.43 (2.56-2.43) |
| Rsym | 0.082 (0.317) | 0.061 (0.122) |
| Total data | 575,380 (71983) | 38,869 (8019) |
| Unique data | 71,520 (10281) | 11,149 (1688) |
| I/σI | 13.4 (4.6) | 14.5 (9.0) |
| Completeness (%) | 99.4 (98.6) | 93.8 (99.5) |
| Redundancy | 8.0 (7.0) | 3.5 (4.8) |