Table 1.
Data collection statistics
| Ligand | KH1060 | MC1288 | 1α,25(OH)2D3 |
|---|---|---|---|
| Space group | P212121 | ||
| Cell dimensions | |||
| a | 44.49 Å | 44.94 Å | 44.93 Å |
| b | 51.87 Å | 51.42 Å | 51.32 Å |
| c | 131.39 Å | 132.52 Å | 132.32 Å |
| Resolution (last shell) | 20–1.52 Å | 15–1.4 Å | 20–1.52 Å |
| (1.56–1.52) | (1.43–1.4) | (1.56–1.52) | |
| Completeness (last shell) | 98.1% (97.3) | 73.4%* (81.1) | 96.2% (66.6) |
| Rsym (last shell) | 4.8% (29) | 4.3% (23.6) | 5% (12.2) |
| 〈I/σ(I)〉 (last shell) | 20.4 (4.6) | 23.4 (3.7) | 20.7 (9.8) |
| Unique reflections | 45,925 | 42,311 | 46,136 |
| Redundancy | 4.8 | 3.6 | 3.4 |
*
See Materials and Methods.