Skip to main content
. Author manuscript; available in PMC: 2013 Feb 20.
Published in final edited form as: Inorg Chem. 2012 Feb 8;51(4):2086–2096. doi: 10.1021/ic2017819

Table 1.

EXAFS Metrics for Split Axial {[Cu(Im)4(Oax1)](Oax2)}·8H2O

CNa R (Å)b σ2×103
4 Neq 2.02±0.002 6.44
1 Oax short 2.12±0.01 13.4
1 Oax long 2.87±0.01 4.18
8 Cα 3.04±0.04 7.94
8 Cβ, Nβ 4.06±0.08 12.5
16 Neq-Cα msc 3.09±0.01 19.7
8 Neq-Nβ ms 4.38±0.13 13.8
16 Cα-Nβ ms 4.22±0.03 2.18
32 Cα-Neq(trans) msd 4.63±0.03 6.76
2 Ow 3.83±0.03 4.62
6 Ow 4.40±0.02 8.67
ΔE0 (eV) −3.533
F-value 0.1237
a

CN=coordination number.

b

uncertainty is the statistical error from the fit.

c

“ms” is multiple scattering. All other interactions are single scattering.

d

triangular multiple scattering path 9; see Figure S7 in the Supporting Information.