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. Author manuscript; available in PMC: 2013 Jan 27.
Published in final edited form as: J Nat Prod. 2011 Dec 12;75(1):60–66. doi: 10.1021/np200611f

Table 1.

1H and 13C NMR Data for Credneramide A (1) and Credneramide B (2).

Credneramide A (1) Credneramide B (2)
carbon δC, mult.a δH, mult. (J in Hz)b HMBCb δC, mult.c δH, mult. (J in Hz)d HMBCd
1 172.1, qC 172.1, qC
2 36.4, CH2 2.19, t (7.0) 1, 3, 4 36.4, CH2 2.22, t (6.9) 1, 3, 4
3 28.4, CH2 2.32, dt (7.0, 6.6) 1, 2, 4, 5 28.5, CH2 2.35, dt (6.9, 6.1) 1, 2, 4, 5
4 131.2, CH 5.43, dt (15.3, 6.6) 2, 5, 6 131.3, CH 5.48, dt (14.9, 6.1) 2, 3, 5, 6
5 127.8, CH 5.47, dt (15.3, 6.7) 3, 4 127.8, CH 5.41, dt (14.9, 6.1) 3, 4, 6, 7
6 37.9, CH2 2.70, d (6.7) 4, 5, 7, 8, 11 37.9, CH2 2.72, d (6.1) 4, 5, 7, 8, 11
7 141.5, qC 141.5, qC
8 32.3, CH2 2.15, t (6.7) 6, 7, 9, 10, 11 32.2, CH2 2.15, t (7.6) 6, 7, 9, 10, 11
9 20.2, CH2 1.43 h (7.5) 7, 8, 10 20.2, CH2 1.43, h (7.6) 7, 8, 10
10 13.9, CH3 0.91 t (7.5) 8, 9 13.9, CH3 0.91, m 8, 9
11 113.1, CH 5.77, s 6, 7, 8 113.1, CH 5.78, s 6, 7, 8, 9
NH 5.42 d (6.2) 5.39
1′ 40.5, CH2 3.53 (dt (6.9, 6.2) 1, 2′, 3′ 37.8, CH2 3.26, dt (7.2, 6.5) 1, 2′, 3′
2′ 35.7, CH2 2.81, t (6.9) 1′, 3′, 4′ 38.5, CH2 1.36, dt (7.5, 7.2) 1′, 3′, 4′, 5′
3′ 138.9, qC 25.9, CH 1.60, m 2′, 4′, 5′
4′ 128.7, CH 7.19, d (7.2) 2′, 5′, 6′, 7′ 22.4, CH3 0.90, m 3′, 5′
5′ 128.7, CH 7.32, dd (7.2) 3′, 4′ 22.4, CH3 0.90, m 3′, 4′
6′ 128.5, CH 7.24, t (7.2) 4′
7′ 128.7, CH 7.32, t (7.2) 3′, 4′
8′ 128.7, CH 7.19, d (7.2) 2′, 5′, 6′, 7′
a

75 MHz in CDCl3.

b

500 MHz in CDCl3.

c

150 MHz CDCl3.

d

600 MHz in CDCl3.