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. 2012 Mar 28;134(14):6409–6415. doi: 10.1021/ja300654t

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Copyright © 2012 American Chemical Society

This is an open-access article distributed under the ACS AuthorChoice Terms & Conditions. Any use of this article, must conform to the terms of that license which are available at http://pubs.acs.org.

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Molecular structure of 4 (thermal ellipsoid plot drawn at the 30% probability level). Hydrogen atoms omitted for clarity (bond lengths in pm, angles in deg). Pb(1)–Si(4) 270.9(4), Pb(1)–Si(1) 273.2(3), Pb(1)–Pb(2) 306.40(8), Pb(2)–Si(12) 269.7(3), Pb(2)–Si(9) 273.7(3), Si(1)–Si(2) 233.4(6), Si(2)–C(1) 187.5(13), Si(4)–Pb(1)–Si(1) 94.38(12), Si(4)–Pb(1)–Pb(2) 109.54(11), Si(1)–Pb(1)–Pb(2) 101.83(7), Si(12)–Pb(2)–Si(9) 96.49(10), Si(12)–Pb(2)–Pb(1) 101.80(7), Si(9)–Pb(2)–Pb(1) 156.09(9).