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. 2012 Feb 24;287(17):13996–14003. doi: 10.1074/jbc.M112.346924

TABLE 1.

Previously reported and currently proposed estimated rates of O-acetylation of corresponding sites in Fig. 1

Previous study (15)
Current study
9V 9A 9V 9A
R1 0.04a 0 0.004 0.005
R2 0.03 0 0.001 0.002
R3 0.25 0 0.55 0.61
R4 0.17 0 0.25 0.27
R5 0.06 0 0.09 0.03
R6 0.55 0 1.04 0
Sumb 1.1 0 1.95 0.92
OAc:NAcc 1.19:1 0:1 1.97:1 1.03:1

a Values are expressed as molar equivalents.

b Sum of all O-acetylation sites according to integration of resolved peaks in 1H NMR spectra.

c Molar ratio of O-acetate to N-acetate according to integration of acetate proton signals in 1H NMR spectra.