TABLE 1.
Previous study (15) |
Current study |
|||
---|---|---|---|---|
9V | 9A | 9V | 9A | |
R1 | 0.04a | 0 | 0.004 | 0.005 |
R2 | 0.03 | 0 | 0.001 | 0.002 |
R3 | 0.25 | 0 | 0.55 | 0.61 |
R4 | 0.17 | 0 | 0.25 | 0.27 |
R5 | 0.06 | 0 | 0.09 | 0.03 |
R6 | 0.55 | 0 | 1.04 | 0 |
Sumb | 1.1 | 0 | 1.95 | 0.92 |
OAc:NAcc | 1.19:1 | 0:1 | 1.97:1 | 1.03:1 |
a Values are expressed as molar equivalents.
b Sum of all O-acetylation sites according to integration of resolved peaks in 1H NMR spectra.
c Molar ratio of O-acetate to N-acetate according to integration of acetate proton signals in 1H NMR spectra.