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. Author manuscript; available in PMC: 2012 May 2.
Published in final edited form as: Angew Chem Int Ed Engl. 2009;48(31):5586–5587. doi: 10.1002/anie.200902237

Table 1.

N-Arylation in the presence of FeCI3 (pyrrazole). graphic file with name nihms-368808-t0001.jpg

FeCI3 3C Yield (%)
>98% (Merck) 87 (ref. 3a)
>98% (Aldrich) 26
>99.99 (Aldrich) 9
>99.99% + 5 ppm Cu2O 78
>99.99% + 10 ppm Cu2O 79
no Fe + ligand + 5 ppm Cu2O 77
no Fe + no ligand + 5 ppm Cu2O 23