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. Author manuscript; available in PMC: 2013 May 2.
Published in final edited form as: J Am Chem Soc. 2012 Apr 24;134(17):7293–7296. doi: 10.1021/ja3019324

Figure 3.

Figure 3

(a) X-band EPR spectrum of 4 collected at 120 K in a 2:3 MeCN:toluene glass (solid black) and the calculated fit (dotted red; displaced vertically from the experimental). (b) CVs of 2 in the absence (yellow) and presence (purple) of 1 equiv [pyH]OTf at -20 °C in 0.25 M [nBu4N]PF6 in MeCN, with scan-rates of 100 mV s-1.