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. 2012 Mar 3;68(Pt 4):m370. doi: 10.1107/S1600536812008513
Bruker SMART CCD area-detector diffractometer 2146 independent reflections
Radiation source: fine-focus sealed tube 1999 reflections with I > 2σ(I)
Graphite Monochromator monochromator Rint = 0.018
phi and ω scans θmax = 29.6°, θmin = 3.5°
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) h = −25→25
Tmin = 0.919, Tmax = 0.938 k = −5→4
7387 measured reflections l = −15→15