C39—O5 | 1.471 (7) | C8—C7 | 1.434 (4) |
C39—H39A | 0.9600 | C14—C15 | 1.394 (6) |
C39—H39B | 0.9600 | C14—H14 | 0.9300 |
C39—H39C | 0.9600 | C36—C37 | 1.380 (4) |
O1—N7 | 1.195 (6) | C36—C35 | 1.383 (4) |
O2—N7 | 1.212 (5) | C36—N10 | 1.451 (4) |
Ni1—N5 | 2.056 (3) | C35—C34 | 1.372 (4) |
Ni1—N8 | 2.062 (3) | C35—H35 | 0.9300 |
Ni1—N4 | 2.076 (2) | C34—H34 | 0.9300 |
Ni1—N1 | 2.097 (2) | C37—H37 | 0.9300 |
Ni1—N3 | 2.098 (2) | C23—H23 | 0.9300 |
Ni1—N2 | 2.139 (2) | C2—C3 | 1.397 (4) |
N2—C11 | 1.323 (3) | C2—H2 | 0.9300 |
N2—C12 | 1.358 (3) | C3—C4 | 1.360 (5) |
N3—C14 | 1.326 (4) | C3—H3 | 0.9300 |
N3—C13 | 1.351 (4) | C19—C18 | 1.340 (6) |
N1—C2 | 1.325 (4) | C19—H19 | 0.9300 |
N1—C1 | 1.358 (3) | C9—C10 | 1.362 (5) |
N4—C23 | 1.322 (4) | C9—H9 | 0.9300 |
N4—C24 | 1.352 (4) | C21—H21 | 0.9300 |
N8—C32 | 1.157 (4) | C17—C16 | 1.390 (6) |
N5—C25 | 1.156 (4) | C17—C18 | 1.438 (6) |
C12—C8 | 1.402 (4) | C10—H10 | 0.9300 |
C12—C1 | 1.435 (4) | O3—N10 | 1.224 (4) |
C5—C4 | 1.402 (5) | N10—O4 | 1.215 (4) |
C5—C1 | 1.405 (4) | C4—H4 | 0.9300 |
C5—C6 | 1.433 (5) | C7—H7 | 0.9300 |
C24—C20 | 1.404 (4) | C18—H18 | 0.9300 |
C24—C13 | 1.432 (4) | C15—C16 | 1.360 (7) |
C13—C17 | 1.407 (4) | C15—H15 | 0.9300 |
C11—C10 | 1.390 (4) | C16—H16 | 0.9300 |
C11—H11 | 0.9300 | N6—C25 | 1.289 (4) |
C20—C21 | 1.403 (6) | N6—C26 | 1.373 (4) |
C20—C19 | 1.425 (6) | C26—C31 | 1.388 (5) |
C6—C7 | 1.342 (5) | C26—C27 | 1.406 (4) |
C6—H6 | 0.9300 | C31—C30 | 1.368 (5) |
N9—C32 | 1.297 (4) | C31—H31 | 0.9300 |
N9—C33 | 1.383 (3) | C30—C29 | 1.380 (5) |
C38—C37 | 1.378 (4) | C30—H30 | 0.9300 |
C38—C33 | 1.402 (4) | C29—C28 | 1.368 (6) |
C38—H38 | 0.9300 | C29—N7 | 1.451 (5) |
C22—C21 | 1.350 (6) | C27—C28 | 1.363 (6) |
C22—C23 | 1.395 (4) | C27—H27 | 0.9300 |
C22—H22 | 0.9300 | C28—H28 | 0.9300 |
C33—C34 | 1.402 (4) | O5—H5A | 0.91 (3) |
C8—C9 | 1.401 (5) | ||
O5—C39—H39A | 109.5 | C37—C36—N10 | 119.4 (3) |
O5—C39—H39B | 109.5 | C35—C36—N10 | 119.3 (3) |
H39A—C39—H39B | 109.5 | C34—C35—C36 | 119.5 (3) |
O5—C39—H39C | 109.5 | C34—C35—H35 | 120.2 |
H39A—C39—H39C | 109.5 | C36—C35—H35 | 120.2 |
H39B—C39—H39C | 109.5 | C35—C34—C33 | 120.9 (3) |
N5—Ni1—N8 | 90.67 (12) | C35—C34—H34 | 119.6 |
N5—Ni1—N4 | 94.32 (10) | C33—C34—H34 | 119.6 |
N8—Ni1—N4 | 92.39 (10) | C38—C37—C36 | 119.1 (3) |
N5—Ni1—N1 | 93.16 (10) | C38—C37—H37 | 120.4 |
N8—Ni1—N1 | 89.69 (10) | C36—C37—H37 | 120.4 |
N4—Ni1—N1 | 172.22 (9) | N4—C23—C22 | 122.5 (3) |
N5—Ni1—N3 | 89.86 (11) | N4—C23—H23 | 118.7 |
N8—Ni1—N3 | 171.74 (10) | C22—C23—H23 | 118.7 |
N4—Ni1—N3 | 79.35 (10) | N1—C2—C3 | 122.6 (3) |
N1—Ni1—N3 | 98.51 (10) | N1—C2—H2 | 118.7 |
N5—Ni1—N2 | 171.53 (9) | C3—C2—H2 | 118.7 |
N8—Ni1—N2 | 91.08 (10) | C4—C3—C2 | 119.5 (3) |
N4—Ni1—N2 | 93.89 (9) | C4—C3—H3 | 120.3 |
N1—Ni1—N2 | 78.56 (9) | C2—C3—H3 | 120.3 |
N3—Ni1—N2 | 89.59 (9) | C18—C19—C20 | 121.2 (3) |
C11—N2—C12 | 117.8 (2) | C18—C19—H19 | 119.4 |
C11—N2—Ni1 | 129.65 (19) | C20—C19—H19 | 119.4 |
C12—N2—Ni1 | 112.50 (17) | C10—C9—C8 | 119.4 (3) |
C14—N3—C13 | 118.2 (3) | C10—C9—H9 | 120.3 |
C14—N3—Ni1 | 129.1 (2) | C8—C9—H9 | 120.3 |
C13—N3—Ni1 | 112.70 (19) | C22—C21—C20 | 119.9 (3) |
C2—N1—C1 | 118.3 (2) | C22—C21—H21 | 120.1 |
C2—N1—Ni1 | 127.8 (2) | C20—C21—H21 | 120.1 |
C1—N1—Ni1 | 113.33 (17) | C16—C17—C13 | 117.1 (4) |
C23—N4—C24 | 118.1 (2) | C16—C17—C18 | 124.5 (4) |
C23—N4—Ni1 | 128.3 (2) | C13—C17—C18 | 118.4 (4) |
C24—N4—Ni1 | 113.61 (18) | C9—C10—C11 | 119.6 (3) |
C32—N8—Ni1 | 150.6 (3) | C9—C10—H10 | 120.2 |
C25—N5—Ni1 | 153.2 (2) | C11—C10—H10 | 120.2 |
N2—C12—C8 | 122.8 (3) | O4—N10—O3 | 122.2 (3) |
N2—C12—C1 | 116.9 (2) | O4—N10—C36 | 118.9 (3) |
C8—C12—C1 | 120.2 (2) | O3—N10—C36 | 118.9 (3) |
C4—C5—C1 | 117.4 (3) | C3—C4—C5 | 119.6 (3) |
C4—C5—C6 | 124.0 (3) | C3—C4—H4 | 120.2 |
C1—C5—C6 | 118.6 (3) | C5—C4—H4 | 120.2 |
N4—C24—C20 | 123.0 (3) | C6—C7—C8 | 121.6 (3) |
N4—C24—C13 | 116.9 (2) | C6—C7—H7 | 119.2 |
C20—C24—C13 | 120.1 (3) | C8—C7—H7 | 119.2 |
N3—C13—C17 | 122.9 (3) | C19—C18—C17 | 121.6 (3) |
N3—C13—C24 | 117.4 (2) | C19—C18—H18 | 119.2 |
C17—C13—C24 | 119.7 (3) | C17—C18—H18 | 119.2 |
N2—C11—C10 | 123.1 (3) | C16—C15—C14 | 119.6 (4) |
N2—C11—H11 | 118.5 | C16—C15—H15 | 120.2 |
C10—C11—H11 | 118.5 | C14—C15—H15 | 120.2 |
C21—C20—C24 | 116.8 (3) | C15—C16—C17 | 119.9 (4) |
C21—C20—C19 | 124.3 (3) | C15—C16—H16 | 120.0 |
C24—C20—C19 | 118.9 (4) | C17—C16—H16 | 120.0 |
C7—C6—C5 | 121.4 (3) | C25—N6—C26 | 117.3 (3) |
C7—C6—H6 | 119.3 | N5—C25—N6 | 176.2 (4) |
C5—C6—H6 | 119.3 | N6—C26—C31 | 124.4 (3) |
N1—C1—C5 | 122.5 (3) | N6—C26—C27 | 118.0 (3) |
N1—C1—C12 | 117.7 (2) | C31—C26—C27 | 117.6 (3) |
C5—C1—C12 | 119.8 (3) | C30—C31—C26 | 121.5 (3) |
C32—N9—C33 | 117.8 (2) | C30—C31—H31 | 119.2 |
C37—C38—C33 | 121.1 (3) | C26—C31—H31 | 119.2 |
C37—C38—H38 | 119.4 | C31—C30—C29 | 119.3 (4) |
C33—C38—H38 | 119.4 | C31—C30—H30 | 120.3 |
C21—C22—C23 | 119.7 (3) | C29—C30—H30 | 120.3 |
C21—C22—H22 | 120.2 | C28—C29—C30 | 120.6 (4) |
C23—C22—H22 | 120.2 | C28—C29—N7 | 120.2 (4) |
N9—C33—C38 | 123.8 (3) | C30—C29—N7 | 119.2 (4) |
N9—C33—C34 | 118.1 (3) | C28—C27—C26 | 120.7 (4) |
C38—C33—C34 | 118.1 (3) | C28—C27—H27 | 119.6 |
C9—C8—C12 | 117.4 (3) | C26—C27—H27 | 119.6 |
C9—C8—C7 | 124.3 (3) | O1—N7—O2 | 122.1 (5) |
C12—C8—C7 | 118.3 (3) | O1—N7—C29 | 118.6 (5) |
N3—C14—C15 | 122.3 (4) | O2—N7—C29 | 119.4 (4) |
N3—C14—H14 | 118.9 | C27—C28—C29 | 120.2 (3) |
C15—C14—H14 | 118.9 | C27—C28—H28 | 119.9 |
N8—C32—N9 | 175.6 (3) | C29—C28—H28 | 119.9 |
C37—C36—C35 | 121.2 (3) | C39—O5—H5A | 104 (4) |
N8—Ni1—N2—C11 | 94.1 (3) | N2—C12—C1—C5 | 177.1 (3) |
N4—Ni1—N2—C11 | 1.6 (3) | C8—C12—C1—C5 | −3.2 (4) |
N1—Ni1—N2—C11 | −176.5 (3) | C32—N9—C33—C38 | 1.2 (4) |
N3—Ni1—N2—C11 | −77.7 (3) | C32—N9—C33—C34 | −178.9 (3) |
N8—Ni1—N2—C12 | −82.19 (19) | C37—C38—C33—N9 | 179.3 (3) |
N4—Ni1—N2—C12 | −174.66 (18) | C37—C38—C33—C34 | −0.6 (4) |
N1—Ni1—N2—C12 | 7.27 (18) | N2—C12—C8—C9 | 2.0 (4) |
N3—Ni1—N2—C12 | 106.04 (19) | C1—C12—C8—C9 | −177.7 (3) |
N5—Ni1—N3—C14 | 83.3 (3) | N2—C12—C8—C7 | −176.8 (3) |
N4—Ni1—N3—C14 | 177.7 (3) | C1—C12—C8—C7 | 3.5 (4) |
N1—Ni1—N3—C14 | −9.9 (3) | C13—N3—C14—C15 | −1.6 (5) |
N2—Ni1—N3—C14 | −88.2 (3) | Ni1—N3—C14—C15 | 179.4 (3) |
N5—Ni1—N3—C13 | −95.8 (2) | C37—C36—C35—C34 | 0.3 (5) |
N4—Ni1—N3—C13 | −1.39 (19) | N10—C36—C35—C34 | −178.1 (3) |
N1—Ni1—N3—C13 | 171.02 (19) | C36—C35—C34—C33 | −0.4 (5) |
N2—Ni1—N3—C13 | 92.6 (2) | N9—C33—C34—C35 | −179.4 (3) |
N5—Ni1—N1—C2 | 2.2 (3) | C38—C33—C34—C35 | 0.5 (5) |
N8—Ni1—N1—C2 | −88.5 (3) | C33—C38—C37—C36 | 0.6 (5) |
N3—Ni1—N1—C2 | 92.5 (3) | C35—C36—C37—C38 | −0.4 (5) |
N2—Ni1—N1—C2 | −179.6 (3) | N10—C36—C37—C38 | 178.0 (3) |
N5—Ni1—N1—C1 | 172.90 (19) | C24—N4—C23—C22 | −0.4 (4) |
N8—Ni1—N1—C1 | 82.2 (2) | Ni1—N4—C23—C22 | −179.9 (2) |
N3—Ni1—N1—C1 | −96.77 (19) | C21—C22—C23—N4 | 1.7 (5) |
N2—Ni1—N1—C1 | −8.92 (18) | C1—N1—C2—C3 | −1.0 (5) |
N5—Ni1—N4—C23 | −89.7 (3) | Ni1—N1—C2—C3 | 169.4 (3) |
N8—Ni1—N4—C23 | 1.1 (3) | N1—C2—C3—C4 | 0.0 (5) |
N3—Ni1—N4—C23 | −178.8 (3) | C21—C20—C19—C18 | 177.8 (4) |
N2—Ni1—N4—C23 | 92.4 (3) | C24—C20—C19—C18 | −1.1 (6) |
N5—Ni1—N4—C24 | 90.8 (2) | C12—C8—C9—C10 | −1.3 (5) |
N8—Ni1—N4—C24 | −178.4 (2) | C7—C8—C9—C10 | 177.4 (3) |
N3—Ni1—N4—C24 | 1.73 (18) | C23—C22—C21—C20 | −1.6 (6) |
N2—Ni1—N4—C24 | −87.13 (19) | C24—C20—C21—C22 | 0.2 (5) |
N5—Ni1—N8—C32 | −33.3 (5) | C19—C20—C21—C22 | −178.6 (4) |
N4—Ni1—N8—C32 | −127.6 (5) | N3—C13—C17—C16 | −0.5 (5) |
N1—Ni1—N8—C32 | 59.9 (5) | C24—C13—C17—C16 | 179.1 (3) |
N2—Ni1—N8—C32 | 138.4 (5) | N3—C13—C17—C18 | 179.4 (3) |
N8—Ni1—N5—C25 | −67.7 (6) | C24—C13—C17—C18 | −1.0 (4) |
N4—Ni1—N5—C25 | 24.7 (6) | C8—C9—C10—C11 | −0.2 (5) |
N1—Ni1—N5—C25 | −157.5 (6) | N2—C11—C10—C9 | 1.2 (5) |
N3—Ni1—N5—C25 | 104.0 (6) | C37—C36—N10—O4 | −2.7 (5) |
C11—N2—C12—C8 | −1.1 (4) | C35—C36—N10—O4 | 175.7 (3) |
Ni1—N2—C12—C8 | 175.6 (2) | C37—C36—N10—O3 | 178.6 (3) |
C11—N2—C12—C1 | 178.6 (2) | C35—C36—N10—O3 | −2.9 (5) |
Ni1—N2—C12—C1 | −4.7 (3) | C2—C3—C4—C5 | 1.0 (5) |
C23—N4—C24—C20 | −1.0 (4) | C1—C5—C4—C3 | −1.0 (5) |
Ni1—N4—C24—C20 | 178.6 (2) | C6—C5—C4—C3 | 178.2 (3) |
C23—N4—C24—C13 | 178.6 (3) | C5—C6—C7—C8 | −1.5 (6) |
Ni1—N4—C24—C13 | −1.8 (3) | C9—C8—C7—C6 | −179.9 (4) |
C14—N3—C13—C17 | 1.2 (4) | C12—C8—C7—C6 | −1.2 (5) |
Ni1—N3—C13—C17 | −179.5 (2) | C20—C19—C18—C17 | 0.7 (6) |
C14—N3—C13—C24 | −178.3 (3) | C16—C17—C18—C19 | −179.8 (4) |
Ni1—N3—C13—C24 | 0.9 (3) | C13—C17—C18—C19 | 0.4 (6) |
N4—C24—C13—N3 | 0.6 (4) | N3—C14—C15—C16 | 1.1 (6) |
C20—C24—C13—N3 | −179.8 (3) | C14—C15—C16—C17 | −0.3 (6) |
N4—C24—C13—C17 | −179.0 (3) | C13—C17—C16—C15 | 0.0 (6) |
C20—C24—C13—C17 | 0.6 (4) | C18—C17—C16—C15 | −179.9 (4) |
C12—N2—C11—C10 | −0.5 (4) | C26—N6—C25—N5 | 177 (100) |
Ni1—N2—C11—C10 | −176.6 (2) | C25—N6—C26—C31 | 6.4 (5) |
N4—C24—C20—C21 | 1.1 (4) | C25—N6—C26—C27 | −172.4 (3) |
C13—C24—C20—C21 | −178.5 (3) | N6—C26—C31—C30 | −177.7 (3) |
N4—C24—C20—C19 | 180.0 (3) | C27—C26—C31—C30 | 1.1 (5) |
C13—C24—C20—C19 | 0.4 (4) | C26—C31—C30—C29 | −0.4 (5) |
C4—C5—C6—C7 | −177.4 (4) | C31—C30—C29—C28 | −0.2 (6) |
C1—C5—C6—C7 | 1.8 (5) | C31—C30—C29—N7 | −178.1 (4) |
C2—N1—C1—C5 | 0.9 (4) | N6—C26—C27—C28 | 177.7 (4) |
Ni1—N1—C1—C5 | −170.8 (2) | C31—C26—C27—C28 | −1.2 (6) |
C2—N1—C1—C12 | −178.9 (3) | C28—C29—N7—O1 | 7.7 (8) |
Ni1—N1—C1—C12 | 9.5 (3) | C30—C29—N7—O1 | −174.4 (6) |
C4—C5—C1—N1 | 0.1 (4) | C28—C29—N7—O2 | −172.6 (5) |
C6—C5—C1—N1 | −179.2 (3) | C30—C29—N7—O2 | 5.3 (7) |
C4—C5—C1—C12 | 179.8 (3) | C26—C27—C28—C29 | 0.6 (7) |
C6—C5—C1—C12 | 0.6 (4) | C30—C29—C28—C27 | 0.1 (7) |
N2—C12—C1—N1 | −3.2 (4) | N7—C29—C28—C27 | 178.0 (4) |
C8—C12—C1—N1 | 176.5 (3) |