| Stoe IPDS II diffractometer | 9512 independent reflections |
| Radiation source: fine-focus sealed tube | 6693 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.053 |
| Detector resolution: 0.15 mm pixels mm-1 | θmax = 29.2°, θmin = 2.1° |
| rotation method scans | h = −12→13 |
| Absorption correction: numerical (X-RED and X-SHAPE; Stoe & Cie, 2005) | k = −15→15 |
| Tmin = 0.862, Tmax = 0.938 | l = −22→20 |
| 19823 measured reflections |
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