Refinement on F2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.061	Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.139	H atoms treated by a mixture of independent and constrained refinement
S = 1.06	w = 1/[σ2(Fo2) + (0.0512P)2 + 0.8996P] where P = (Fo2 + 2Fc2)/3
9512 reflections	(Δ/σ)max = 0.001
501 parameters	Δρmax = 0.65 e Å−3
1 restraint	Δρmin = −0.31 e Å−3