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. 2012 Mar 3;68(Pt 4):o932. doi: 10.1107/S1600536812008124
C1—C9A 1.394 (5) C9—C10 1.352 (5)
C1—C2 1.395 (5) C9—C9A 1.482 (5)
C1—H1A 0.9300 C10—C13 1.436 (6)
C2—C3 1.386 (6) C10—C11 1.442 (6)
C2—H2A 0.9300 C11—N12 1.144 (5)
C3—C4 1.382 (6) C13—N14 1.147 (5)
C3—H3A 0.9300 S15—C16 1.722 (6)
C4—C4A 1.386 (5) S15—C19 1.752 (4)
C4—H4A 0.9300 C16—C17 1.312 (6)
C4A—C9A 1.404 (5) C16—H16A 0.9300
C4A—C4B 1.460 (6) C17—S18 1.737 (5)
C4B—C5 1.386 (5) C17—H17A 0.9300
C4B—C8A 1.421 (5) S18—C19 1.762 (4)
C5—C6 1.384 (6) C19—C19i 1.351 (8)
C5—H5A 0.9300 S20—C21 1.726 (5)
C6—C7 1.378 (6) S20—C24 1.759 (4)
C6—H6A 0.9300 C21—C22 1.317 (6)
C7—C8 1.392 (5) C21—H21A 0.9300
C7—H7A 0.9300 C22—S23 1.734 (4)
C8—C8A 1.388 (5) C22—H22A 0.9300
C8—H8A 0.9300 S23—C24 1.766 (4)
C8A—C9 1.483 (5) C24—C24ii 1.324 (7)
C9A—C1—C2 118.5 (4) C10—C9—C9A 127.4 (4)
C9A—C1—H1A 120.8 C10—C9—C8A 126.8 (4)
C2—C1—H1A 120.8 C9A—C9—C8A 105.8 (3)
C3—C2—C1 120.4 (4) C1—C9A—C4A 120.6 (4)
C3—C2—H2A 119.8 C1—C9A—C9 130.8 (4)
C1—C2—H2A 119.8 C4A—C9A—C9 108.5 (4)
C4—C3—C2 121.2 (4) C9—C10—C13 123.1 (4)
C4—C3—H3A 119.4 C9—C10—C11 123.8 (4)
C2—C3—H3A 119.4 C13—C10—C11 113.1 (4)
C3—C4—C4A 119.1 (4) N12—C11—C10 177.1 (5)
C3—C4—H4A 120.4 N14—C13—C10 178.0 (5)
C4A—C4—H4A 120.4 C16—S15—C19 94.7 (2)
C4—C4A—C9A 120.1 (4) C17—C16—S15 118.3 (5)
C4—C4A—C4B 130.7 (4) C17—C16—H16A 120.9
C9A—C4A—C4B 109.2 (4) S15—C16—H16A 120.9
C5—C4B—C8A 120.8 (4) C16—C17—S18 118.5 (5)
C5—C4B—C4A 131.0 (4) C16—C17—H17A 120.8
C8A—C4B—C4A 108.2 (4) S18—C17—H17A 120.8
C6—C5—C4B 118.1 (4) C17—S18—C19 93.8 (2)
C6—C5—H5A 120.9 C19i—C19—S15 123.0 (5)
C4B—C5—H5A 120.9 C19i—C19—S18 122.5 (5)
C7—C6—C5 122.2 (4) S15—C19—S18 114.6 (2)
C7—C6—H6A 118.9 C21—S20—C24 94.8 (2)
C5—C6—H6A 118.9 C22—C21—S20 118.2 (4)
C6—C7—C8 119.9 (4) C22—C21—H21A 120.9
C6—C7—H7A 120.1 S20—C21—H21A 120.9
C8—C7—H7A 120.1 C21—C22—S23 118.4 (4)
C8A—C8—C7 119.7 (4) C21—C22—H22A 120.8
C8A—C8—H8A 120.1 S23—C22—H22A 120.8
C7—C8—H8A 120.1 C22—S23—C24 94.4 (2)
C8—C8A—C4B 119.3 (4) C24ii—C24—S20 123.1 (4)
C8—C8A—C9 132.4 (4) C24ii—C24—S23 122.8 (4)
C4B—C8A—C9 108.3 (4) S20—C24—S23 114.1 (2)
C9A—C1—C2—C3 −0.1 (6) C4—C4A—C9A—C1 0.4 (6)
C1—C2—C3—C4 0.5 (7) C4B—C4A—C9A—C1 178.9 (3)
C2—C3—C4—C4A −0.3 (7) C4—C4A—C9A—C9 −177.2 (4)
C3—C4—C4A—C9A −0.1 (6) C4B—C4A—C9A—C9 1.3 (4)
C3—C4—C4A—C4B −178.2 (4) C10—C9—C9A—C1 1.4 (6)
C4—C4A—C4B—C5 −2.0 (7) C8A—C9—C9A—C1 −178.0 (4)
C9A—C4A—C4B—C5 179.7 (4) C10—C9—C9A—C4A 178.7 (4)
C4—C4A—C4B—C8A 176.8 (4) C8A—C9—C9A—C4A −0.7 (4)
C9A—C4A—C4B—C8A −1.4 (4) C9A—C9—C10—C13 −176.9 (4)
C8A—C4B—C5—C6 −1.5 (6) C8A—C9—C10—C13 2.3 (6)
C4A—C4B—C5—C6 177.3 (4) C9A—C9—C10—C11 3.1 (6)
C4B—C5—C6—C7 1.9 (6) C8A—C9—C10—C11 −177.6 (3)
C5—C6—C7—C8 −1.1 (6) C19—S15—C16—C17 1.9 (5)
C6—C7—C8—C8A −0.2 (6) S15—C16—C17—S18 0.8 (6)
C7—C8—C8A—C4B 0.6 (5) C16—C17—S18—C19 −3.0 (5)
C7—C8—C8A—C9 −179.0 (4) C16—S15—C19—C19i 175.8 (5)
C5—C4B—C8A—C8 0.3 (5) C16—S15—C19—S18 −3.9 (3)
C4A—C4B—C8A—C8 −178.7 (3) C17—S18—C19—C19i −175.6 (5)
C5—C4B—C8A—C9 179.9 (3) C17—S18—C19—S15 4.2 (3)
C4A—C4B—C8A—C9 0.9 (4) C24—S20—C21—C22 1.5 (4)
C8—C8A—C9—C10 0.1 (6) S20—C21—C22—S23 0.1 (6)
C4B—C8A—C9—C10 −179.5 (4) C21—C22—S23—C24 −1.5 (4)
C8—C8A—C9—C9A 179.4 (4) C21—S20—C24—C24ii 178.3 (5)
C4B—C8A—C9—C9A −0.2 (4) C21—S20—C24—S23 −2.4 (3)
C2—C1—C9A—C4A −0.3 (6) C22—S23—C24—C24ii −178.3 (5)
C2—C1—C9A—C9 176.7 (4) C22—S23—C24—S20 2.4 (3)