| Bruker P4 diffractometer | 1541 reflections with I > 2σ(I) |
| Radiation source: X-ray | Rint = 0.062 |
| Graphite monochromator | θmax = 25.0°, θmin = 2.3° |
| 2θ/ω scans | h = −9→3 |
| Absorption correction: ψ scan (XSCANS; Siemens, 1996) | k = −10→10 |
| Tmin = 0.650, Tmax = 0.688 | l = −16→16 |
| 5766 measured reflections | 2 standard reflections every 48 reflections |
| 3493 independent reflections | intensity decay: 14% |