| Stoe IPDS 2 diffractometer | 4737 independent reflections |
| Radiation source: fine-focus sealed tube | 1740 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.105 |
| Detector resolution: 6.67 pixels mm-1 | θmax = 26.3°, θmin = 1.2° |
| rotation method scans | h = −7→7 |
| Absorption correction: integration (X-RED32; Stoe & Cie, 2002) | k = −41→41 |
| Tmin = 0.967, Tmax = 0.994 | l = −15→15 |
| 26921 measured reflections |