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. 2012 Mar 14;68(Pt 4):o1052. doi: 10.1107/S1600536812010203
Stoe IPDS 2 diffractometer 4737 independent reflections
Radiation source: fine-focus sealed tube 1740 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.105
Detector resolution: 6.67 pixels mm-1 θmax = 26.3°, θmin = 1.2°
rotation method scans h = −7→7
Absorption correction: integration (X-RED32; Stoe & Cie, 2002) k = −41→41
Tmin = 0.967, Tmax = 0.994 l = −15→15
26921 measured reflections