Experimental. Intensity data was collected on a Bruker X8 Apex II 4 K Kappa CCD diffractometer using an exposure time of 55 s/frame. A total of 1495 frames were collected with a frame width of 0.5° covering up to θ = 28.0° with 99.6% completeness accomplished

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.