| Stoe IPDS diffractometer | 2244 independent reflections |
| Radiation source: normal-focus sealed tube | 1662 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.037 |
| Detector resolution: 6.66 pixels mm-1 | θmax = 25.8°, θmin = 2.0° |
| 0.6° φ scans | h = −50→50 |
| Absorption correction: gaussian (PLATON-ABSGAUSS; Spek, 2009) | k = −5→5 |
| Tmin = 0.953, Tmax = 0.993 | l = −14→15 |
| 10694 measured reflections |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.