Bruker SMART CCD-detector diffractometer | 7775 independent reflections |
Radiation source: fine-focus sealed tube | 7155 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.028 |
φ and ω scans | θmax = 27.0°, θmin = 1.0° |
Absorption correction: multi-scan (SADABS; Bruker, 2000) | h = −11→11 |
Tmin = 0.617, Tmax = 0.807 | k = −13→13 |
30524 measured reflections | l = −25→25 |