| Bruker SMART 1000 CCD diffractometer | 3126 independent reflections |
| Radiation source: fine-focus sealed tube | 2612 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.018 |
| φ and ω scans | θmax = 26.0°, θmin = 2.1° |
| Absorption correction: multi-scan (SADABS; Bruker, 2000) | h = −10→11 |
| Tmin = 0.813, Tmax = 1.000 | k = −11→10 |
| 5100 measured reflections | l = −13→13 |