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. 2012 Apr 13;68(Pt 5):o1343. doi: 10.1107/S1600536812014511
Bruker SMART CCD area-detector diffractometer 1940 independent reflections
Radiation source: fine-focus sealed tube 1184 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.062
phi and ω scans θmax = 25.0°, θmin = 2.0°
Absorption correction: multi-scan (SADABS; Bruker, 2002) h = −12→12
Tmin = 0.957, Tmax = 0.991 k = −13→9
5465 measured reflections l = −11→11