Bruker SMART CCD area-detector diffractometer | 1940 independent reflections |
Radiation source: fine-focus sealed tube | 1184 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.062 |
phi and ω scans | θmax = 25.0°, θmin = 2.0° |
Absorption correction: multi-scan (SADABS; Bruker, 2002) | h = −12→12 |
Tmin = 0.957, Tmax = 0.991 | k = −13→9 |
5465 measured reflections | l = −11→11 |