Bruker SMART APEXII CCD area-detector diffractometer | 3267 independent reflections |
Radiation source: fine-focus sealed tube | 2846 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.000 |
φ and ω scans | θmax = 69.8°, θmin = 7.7° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −15→14 |
Tmin = 0.204, Tmax = 0.923 | k = −12→12 |
3267 measured reflections | l = 0→16 |