Refinement on F2 | Primary atom site location: structure-invariant direct methods |
Least-squares matrix: full | Secondary atom site location: difference Fourier map |
R[F2 > 2σ(F2)] = 0.064 | Hydrogen site location: inferred from neighbouring sites |
wR(F2) = 0.184 | H-atom parameters constrained |
S = 1.13 | w = 1/[σ2(Fo2) + (0.P)2 + 1.1111P] where P = (Fo2 + 2Fc2)/3 |
3267 reflections | (Δ/σ)max = 0.001 |
203 parameters | Δρmax = 0.32 e Å−3 |
0 restraints | Δρmin = −0.37 e Å−3 |