Nonius KappaCCD diffractometer | 4592 independent reflections |
Radiation source: fine-focus sealed tube | 3598 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.055 |
ω and φ scans | θmax = 27.6°, θmin = 2.7° |
Absorption correction: multi-scan (SORTAV; Blessing, 1997) | h = −16→16 |
Tmin = 0.913, Tmax = 0.930 | k = −12→12 |
16108 measured reflections | l = −21→20 |