| Refinement on F2 | Secondary atom site location: difference Fourier map |
| Least-squares matrix: full | Hydrogen site location: inferred from neighbouring sites |
| R[F2 > 2σ(F2)] = 0.047 | H-atom parameters constrained |
| wR(F2) = 0.097 | w = 1/[σ2(Fo2) + (0.0358P)2 + 0.0448P] where P = (Fo2 + 2Fc2)/3 |
| S = 1.06 | (Δ/σ)max < 0.001 |
| 2766 reflections | Δρmax = 0.19 e Å−3 |
| 175 parameters | Δρmin = −0.22 e Å−3 |
| 0 restraints | Absolute structure: assigned from the known absolute structure of the (R)-tert-butanesulfinamide starting material; the Flack (1983) parameter is consistent with this assignment, 1017 Friedel pairs |
| Primary atom site location: structure-invariant direct methods | Flack parameter: 0.03 (10) |