| Oxford Diffraction Xcalibur Ruby Gemini diffractometer | 3188 independent reflections |
| Radiation source: Enhance (Cu) X-ray Source | 2148 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.090 |
| Detector resolution: 10.5081 pixels mm-1 | θmax = 75.8°, θmin = 2.9° |
| ω scans | h = −22→16 |
| Absorption correction: multi-scan (CrysAlis PRO; Oxford Diffraction, 2007) | k = −4→4 |
| Tmin = 0.233, Tmax = 1.000 | l = −23→29 |
| 5147 measured reflections |