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. 2012 Apr 28;68(Pt 5):o1557–o1558. doi: 10.1107/S1600536812018272
Cl1—O3 1.444 (3) C5—H5A 0.9700
Cl1—O2 1.452 (3) C5—H5B 0.9700
Cl1—O1 1.454 (3) C1'—H1'B 0.9600
Cl1—O4 1.775 (4) C1'—H1'C 0.9600
Cl2—O5 1.412 (5) C1'—H1'D 0.9600
Cl2—O7 1.430 (3) C2'—H2'A 0.9600
Cl2—O6 1.464 (5) C2'—H2'B 0.9600
Cl2—O8 1.747 (5) C2'—H2'C 0.9600
Cl3—C18 1.741 (4) C3'—C4' 1.538 (10)
N2—C6 1.318 (4) C3'—H3'A 0.9700
N2—C5 1.450 (5) C3'—H3'B 0.9700
N2—H2D 0.8600 C4'—H4'A 0.9700
N3—C13 1.330 (4) C4'—H4'B 0.9700
N3—C6 1.346 (4) C6—C7 1.461 (5)
N4—C13 1.341 (4) C7—C12 1.398 (5)
N4—C12 1.392 (4) C7—C8 1.400 (5)
N4—H4C 0.8600 C8—C9 1.374 (5)
N5—C13 1.338 (4) C8—H8 0.9300
N5—N6 1.379 (4) C9—C10 1.382 (6)
N5—H5C 0.8600 C9—H9 0.9300
N6—C14 1.272 (4) C10—C11 1.384 (6)
C1—N1 1.517 (7) C10—H10 0.9300
C1—H1B 0.9600 C11—C12 1.404 (5)
C1—H1C 0.9600 C11—H11 0.9300
C1—H1D 0.9600 C14—C15 1.450 (5)
C2—N1 1.430 (16) C14—H14 0.9300
C2—H2A 0.9600 C15—C20 1.400 (5)
C2—H2B 0.9600 C15—C16 1.404 (5)
C2—H2C 0.9600 C16—C17 1.372 (5)
N1—C3 1.465 (6) C16—H16 0.9300
N1—H1A 0.9100 C17—C18 1.386 (5)
C3—C4 1.510 (7) C17—H17 0.9300
C3—H3A 0.9700 C18—C19 1.375 (5)
C3—H3B 0.9700 C19—C20 1.378 (5)
C4—C5 1.620 (7) C19—H19 0.9300
C4—H4A 0.9700 C20—H20 0.9300
C4—H4B 0.9700
O3—Cl1—O2 110.00 (19) H5A—C5—H5B 108.6
O3—Cl1—O1 114.28 (17) H1'B—C1'—H1'C 109.5
O2—Cl1—O1 112.44 (19) H1'B—C1'—H1'D 109.5
O3—Cl1—O4 107.1 (2) H1'C—C1'—H1'D 109.5
O2—Cl1—O4 106.45 (18) H2'A—C2'—H2'B 109.5
O1—Cl1—O4 106.02 (19) H2'A—C2'—H2'C 109.5
O5—Cl2—O7 110.7 (3) H2'B—C2'—H2'C 109.5
O5—Cl2—O6 116.7 (5) C4'—C3'—H3'A 109.0
O7—Cl2—O6 110.9 (3) C4'—C3'—H3'B 109.0
O5—Cl2—O8 105.3 (3) H3'A—C3'—H3'B 107.8
O7—Cl2—O8 107.5 (2) C3'—C4'—H4'A 110.6
O6—Cl2—O8 105.0 (3) C3'—C4'—H4'B 110.6
C6—N2—C5 122.3 (3) H4'A—C4'—H4'B 108.7
C6—N2—H2D 118.8 N2—C6—N3 117.7 (3)
C5—N2—H2D 118.8 N2—C6—C7 120.5 (3)
C13—N3—C6 119.0 (3) N3—C6—C7 121.8 (3)
C13—N4—C12 120.5 (3) C12—C7—C8 119.3 (3)
C13—N4—H4C 119.7 C12—C7—C6 115.8 (3)
C12—N4—H4C 119.7 C8—C7—C6 124.8 (3)
C13—N5—N6 119.2 (3) C9—C8—C7 120.7 (4)
C13—N5—H5C 120.4 C9—C8—H8 119.6
N6—N5—H5C 120.4 C7—C8—H8 119.6
C14—N6—N5 116.2 (3) C8—C9—C10 119.7 (4)
N1—C1—H1B 109.5 C8—C9—H9 120.1
N1—C1—H1C 109.5 C10—C9—H9 120.1
H1B—C1—H1C 109.5 C9—C10—C11 121.2 (4)
N1—C1—H1D 109.5 C9—C10—H10 119.4
H1B—C1—H1D 109.5 C11—C10—H10 119.4
H1C—C1—H1D 109.5 C10—C11—C12 119.2 (4)
N1—C2—H2A 109.5 C10—C11—H11 120.4
N1—C2—H2B 109.5 C12—C11—H11 120.4
H2A—C2—H2B 109.5 N4—C12—C7 119.5 (3)
N1—C2—H2C 109.5 N4—C12—C11 120.8 (3)
H2A—C2—H2C 109.5 C7—C12—C11 119.8 (3)
H2B—C2—H2C 109.5 N3—C13—N5 116.5 (3)
C2—N1—C3 123.2 (6) N3—C13—N4 123.4 (3)
C2—N1—C1 109.2 (6) N5—C13—N4 120.1 (3)
C3—N1—C1 97.5 (5) N6—C14—C15 120.7 (3)
C2—N1—H1A 108.6 N6—C14—H14 119.6
C3—N1—H1A 108.6 C15—C14—H14 119.6
C1—N1—H1A 108.6 C20—C15—C16 118.6 (3)
N1—C3—C4 106.3 (5) C20—C15—C14 120.6 (3)
N1—C3—H3A 110.5 C16—C15—C14 120.8 (3)
C4—C3—H3A 110.5 C17—C16—C15 120.1 (3)
N1—C3—H3B 110.5 C17—C16—H16 119.9
C4—C3—H3B 110.5 C15—C16—H16 119.9
H3A—C3—H3B 108.7 C16—C17—C18 119.4 (3)
C3—C4—C5 113.7 (5) C16—C17—H17 120.3
C3—C4—H4A 108.8 C18—C17—H17 120.3
C5—C4—H4A 108.8 C19—C18—C17 122.2 (3)
C3—C4—H4B 108.8 C19—C18—Cl3 118.9 (3)
C5—C4—H4B 108.8 C17—C18—Cl3 119.0 (3)
H4A—C4—H4B 107.7 C18—C19—C20 118.2 (3)
N2—C5—C4 106.7 (4) C18—C19—H19 120.9
N2—C5—H5A 110.4 C20—C19—H19 120.9
C4—C5—H5A 110.4 C19—C20—C15 121.5 (3)
N2—C5—H5B 110.4 C19—C20—H20 119.3
C4—C5—H5B 110.4 C15—C20—H20 119.3