Table 3.
| ||
---|---|---|
entry | product | yield (%) |
1 |
1a |
95a |
2 |
1b |
89 |
3 |
1c |
91 |
4 |
1d |
92 |
5 |
1e |
91 |
6 |
1f |
90 |
7 |
1g |
93 |
8 |
1h |
92 |
9 |
1i |
88 |
Reaction conditions: 1 mmol of aryltrifluoroborate and NOBF4 (1.03 equiv) in 3 mL of CH3CN for 30 sec at room temperature in an open flask.
5 mmol scale.