Table 1.
Position | 1 a | 2 a | 3 a | 4 a | 5 a | 6 b |
---|---|---|---|---|---|---|
1 | 60.6, CH | 84.0, C | 191.8, C | 197.6, C | 46.2, CH | 82.1, C |
2 | 52.6, C | 62.9, C | 53.1, C | 49.5, C | 63.8, CH | 61.6, C |
3 | 154.0, C | 48.5, CH | 53.1, CH | 52.4, CH | 182.6, C | 47.0, CH |
4 | 197.3, C | 210.5, C | 218.5, C | 214.3, C | 128.4, CH | 210.4, C |
5 | 125.0, CH | 126.9, CH | 34.4, CH2 | 36.4, CH2 | 211.1, C | 116.8, CH |
6 | 186.9, C | 187.5, C | 54.3, CH | 59.5, CH | 61.8, C | 192.3, C |
7 | 43.6, CH2 | 126.2, CH | 67.4, CH | 212.8, C | 76.9, CH | 116.0, CH |
8 | 92.5, C | 158.0, C | 145.2, C | 139.8, C | 49.8, CH | 173.9, C |
9 | 55.9, CH2 | 207.6, C | 209.1, C | 202.6, C | 39.9, CH2 | 75.8, CH |
10 | 43.4, C | 51.0, C | 50.6, C | 51.7, C | 41.3, C | 42.3, C |
11 | 41.2, CH2 | 41.7, CH2 | 40.1, CH2 | 41.0, CH2 | 49.1, CH2 | 44.5, CH2 |
12 | 22.8, CH3 | 22.9, CH3 | 17.6, CH3 | 17.5, CH3 | 15.0, CH3 | 23.9, CH3 |
13 | 113.4, CH2 | 9.5, CH3 | 9.3, CH3 | 9.4, CH3 | 19.7, CH3 | 9.4, CH3 |
14 | 30.2, CH3 | 27.7, CH3 | 25.4, CH3 | 25.2, CH3 | 29.3, CH3 | 29.6, CH3 |
15 | 28.1, CH3 | 26.2, CH3 | 25.0, CH3 | 25.0, CH3 | 29. 2, CH3 | 23.0, CH3 |
a Measured in CDCl3, and CDCl3 was used as an internal standard (δC 77.0); b Measured in DMSO-d6, and DMSO-d6 was used as an internal standard (δC 39.43).