Table 1.
No. | 13C-NMR | 1H-NMR | HMBC |
---|---|---|---|
2 | 78.4 | 5.37 (dd, J = 12.4, 2.9 Hz, 1H) | H-3b, H-2′ or H-6′ |
3 | 42.1 | 2.69 (dd, J = 17.0, 2.9 Hz, 1H) | |
3.18 (dd, J = 17.0, 12.5 Hz, 1H) | |||
4 | 196.2 | H-3a, H3b | |
5 | 162.9 | H-6 | |
6 | 95.8 | 5.88 (d, J = 1.2 Hz, 1H) | 5-OH |
7 | 166.7 | H-6 or H-8 | |
8 | 95.0 | 5.88 (d, J = 1.2 Hz, 1H) | |
9 | 163.4 | H-8, 5-OH | |
10 | 101.7 | H-6 or H-8, 5-OH | |
1′ | 129.4 | H-3b, H-2′ or H-6′ | |
2′ | 117.9 | 6.75 (brs, 1H) | H-4′ |
3′ | 145.7 | H-4′ | |
4′ | 114.3 | 6.88 (brs, 1H) | H-2′ or H-6′ |
5′ | 145.2 | H-4′, H-2′ or H-6′ | |
6′ | 115.3 | 6.75 (brs, 1H) | |
5-OH | 12.14 (s, 1H) | ||
7-OH | 10.76 (s, 1H) | ||
3′-OH | 9.00 (s, 1H) | ||
5′-OH | 9.05 (s, 1H) |