Table 2.
Conducted at room temperature for 20 h in 2 wt% Brij 35/water with 10 mol% Pd(OAc)2, AgOAc (2 equiv), aq. HBF4 (5 equiv), 1 (0.25 mmol), and 2 (2 equiv).
Run for 48 h.
Run for 72 h.
Run for 96 h.
1.2 equiv of ArI.
Conducted at room temperature for 20 h in 2 wt% Brij 35/water with 10 mol% Pd(OAc)2, AgOAc (2 equiv), aq. HBF4 (5 equiv), 1 (0.25 mmol), and 2 (2 equiv).
Run for 48 h.
Run for 72 h.
Run for 96 h.
1.2 equiv of ArI.