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. Author manuscript; available in PMC: 2012 May 30.

Published in final edited form as: Biochemistry. 2011 Nov 3;50(47):10231–10240. doi: 10.1021/bi200801z

Table 3.

Data Collection and Refinement Statistics

	native (Cu anomalous)	Zn anomalous
data collection
wavelength (Å)	1.37765	1.27816
resolution (Å)^a	50–2.68 (2.75–2.68)	50–3.6 (3.66–3.60)
R_sym	0.146 (0.549)	0.201 (0.571)
I/σI	19.2 (1.6)	20.1 (5.3)
completeness (%)	88.9 (54.4)	99.2 (94.3)
redundancy	12.6 (6.8)	12.3 (9.4)
refinement
no. of reflections	83 726
R_work/R_free^b	0.249/0.281
B-factor (Å2)	49.7
rms deviations
bond lengths (Å)	0.016
bond angles (deg)	1.735

^a

Values in parentheses refer to the highest-resolution shell.

^b

For calculation of R_free, 5% of the reflections were reserved.