TABLE 1.
Temperature | Gly NH |
NH (except for Gly NH) |
Pro N | |||||||
---|---|---|---|---|---|---|---|---|---|---|
Peak 1 | Peak 2 | Peak 3 | Peak 4 | Peak 5 | Peak 6 | Peak 7 | ||||
37 °C | ||||||||||
1D, 15N | 107.6a | 110.7 | 117.6 | 119.4 | 121.9 | 133.7 | 135.7 | 138.2 | ||
2D, 15N | 106.3b | 107.3 | 107.9 | 110.6 | 117.4 | 119.3 | 122.1 | |||
2D, 1H | 8.20b | 8.13 | 8.31 | 8.40 | 7.80 | 7.92 | 7.97 | |||
21 °C | ||||||||||
2D, 15N | 106.7b | 107.3 | 108.2 | 111.2 | 117.8 | 120.1 | 122.2 | |||
2D, 1H | 8.26b | 8.15 | 8.33 | 8.46 | 7.84 | 8.02 | 7.95 | |||
5 °C | ||||||||||
1D, 15N | 107.8a | 108.5a | 111.8 | 118.5 | 120.5 | 122.5 | 134.3 | 136.3 | 139.2 | |
2D, 15N | 107.3 | 107.5 | 108.5 | 111.7 | 118.4 | 120.3 | 122.5 | |||
2D, 1H | 8.35 | 8.19 | 8.48 | 8.54 | 7.95 | 8.09 | 8.11 |
a Peaks 1–3 were not well resolved on a one-dimensional spectrum.
b The top of the peak was not apparent on a two-dimensional spectrum.