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Representative decay curves of the hyperpolarized solid-state NMR signal of 100 μL trityl-doped samples (1.4 M [1-13C]pyruvate in 1:1 (v/v) glycerol:water doped with 15 mM trityl OX063) mixed with different concentrations of Gd3+. Inset: 13C solid-state T1 values extracted from the decay curves versus different Gd3+ concentrations.
