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. Author manuscript; available in PMC: 2013 Jun 4.
Published in final edited form as: Mol Pharm. 2012 May 15;9(6):1612–1619. doi: 10.1021/mp200612n

Table 3.

Corrected peak areas and the calculation %RSD for oligosaccharides containing α-1,3-Gal epitopes in the N-glycan pool of the NCI Reference Standard.

NCI Peak Number

Releas
e
10 11 12 13 17 20 23 24 28 29 31 α-1,3-Gal content,
%
1 Corrected peak area
Corrected peak area %
12317
2.09
9404
1.59
5394
0.91
175374
29.71
193566
32.79
55868
9.46
12349
2.09
85985
14.57
15424
2.61
6013
1.02
18650
3.16
9.80

2 Corrected peak area
Corrected peak area %
12885
2.06
10602
1.70
5545
0.89
186217
29.78
204462
32.70
59587
9.53
12865
2.06
90697
14.50
16748
2.68
6330
1.01
19368
3.10
9.73

3 Corrected peak area
Corrected peak area %
9691
2.02
7169
1.49
4370
0.91
142603
29.71
157837
32.88
45510
9.48
10099
2.10
70280
14.64
12405
2.58
4933
1.03
15103
3.15
9.77

4 Corrected peak area
Corrected peak area %
10532
2.00
8431
1.60
4685
0.89
157444
29.84
173171
32.82
50289
9.53
10947
2.08
76785
14.55
13620
2.58
5333
1.01
16345
3.10
9.65

5 Corrected peak area
Corrected peak area %
14333
2.24
10419
1.63
5600
0.87
176665
27.56
219307
34.22
61205
9.55
13207
2.06
97335
15.19
15999
2.50
6594
1.03
20299
3.17
9.63