| Agilent SuperNova Dual diffractometer with an Atlas detector | 5326 independent reflections |
| Radiation source: SuperNova (Mo) X-ray Source | 4445 reflections with I > 2σ(I) |
| Mirror monochromator | Rint = 0.033 |
| Detector resolution: 10.4041 pixels mm-1 | θmax = 27.6°, θmin = 2.6° |
| ω scan | h = −29→40 |
| Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2012) | k = −10→10 |
| Tmin = 0.645, Tmax = 0.856 | l = −26→16 |
| 15316 measured reflections |