Stoe IPDS 2T diffractometer	4014 independent reflections
Radiation source: fine-focus sealed tube	2304 reflections with I > 2σ(I)
Graphite monochromator	Rint = 0.076
Detector resolution: 0.15 mm pixels mm-1	θmax = 29.2°, θmin = 2.2°
rotation method scans	h = −12→12
Absorption correction: numerical [shape of crystal determined optically (X-RED32; Stoe & Cie, (2005)]	k = −23→25
Tmin = 0.274, Tmax = 0.383	l = −12→12
11850 measured reflections