Bruker SMART APEXII DUO CCD area-detector diffractometer | 11176 independent reflections |
Radiation source: fine-focus sealed tube | 11085 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.016 |
φ and ω scans | θmax = 27.5°, θmin = 1.8° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −13→13 |
Tmin = 0.513, Tmax = 0.899 | k = −26→26 |
23611 measured reflections | l = −15→16 |