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. 2012 May 31;68(Pt 6):m847–m848. doi: 10.1107/S1600536812023732
Rigaku Saturn724 CCD diffractometer 3418 independent reflections
Radiation source: rotating anode 1459 reflections with I > 2σ(I)
Multilayer monochromator Rint = 0.106
Detector resolution: 14.22 pixels mm-1 θmax = 25.0°, θmin = 2.4°
ω and φ scans h = −8→8
Absorption correction: multi-scan (CrystalClear; Molecular Structure Corporation & Rigaku, 2005) k = −10→10
Tmin = 0.834, Tmax = 0.985 l = −18→18
8262 measured reflections