Rigaku Saturn724 CCD diffractometer | 3418 independent reflections |
Radiation source: rotating anode | 1459 reflections with I > 2σ(I) |
Multilayer monochromator | Rint = 0.106 |
Detector resolution: 14.22 pixels mm-1 | θmax = 25.0°, θmin = 2.4° |
ω and φ scans | h = −8→8 |
Absorption correction: multi-scan (CrystalClear; Molecular Structure Corporation & Rigaku, 2005) | k = −10→10 |
Tmin = 0.834, Tmax = 0.985 | l = −18→18 |
8262 measured reflections |