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. 2012 May 5;68(Pt 6):o1642. doi: 10.1107/S1600536812018454
F1—C15 1.370 (2) C3—H14 0.974 (19)
N3—C10 1.337 (2) N1—C10 1.314 (3)
N3—N2 1.364 (2) N1—C9 1.358 (3)
N3—C8 1.425 (2) C5—C4 1.383 (3)
O1—C11 1.233 (2) C5—H12 0.980 (19)
C8—C7 1.343 (3) C2—C1 1.385 (3)
C8—C11 1.487 (2) C2—H11 0.976 (19)
C16—C15 1.361 (3) C1—H10 0.99 (2)
C16—C17 1.413 (3) C15—C14 1.377 (3)
C16—H23 0.906 (19) C18—C19 1.524 (3)
C17—N4 1.363 (2) C18—H8A 1.03 (2)
C17—C12 1.422 (2) C18—H8B 1.01 (2)
C12—C13 1.407 (3) C10—H7 0.98 (2)
C12—C11 1.478 (3) C9—H6 0.98 (2)
N2—C9 1.316 (3) C14—H5 0.954 (19)
N4—C18 1.468 (2) C4—H4 0.98 (2)
N4—C21 1.471 (2) C21—C20 1.519 (3)
C13—C14 1.372 (3) C21—H3A 1.026 (18)
C13—H18 0.940 (19) C21—H3B 1.03 (2)
C6—C5 1.394 (3) C20—C19 1.519 (3)
C6—C1 1.406 (3) C20—H2A 0.99 (2)
C6—C7 1.467 (2) C20—H2B 1.01 (2)
C7—H15 1.004 (18) C19—H1A 1.03 (2)
C3—C4 1.378 (3) C19—H1B 0.98 (2)
C3—C2 1.384 (3)
C10—N3—N2 109.69 (16) C2—C1—H10 119.7 (11)
C10—N3—C8 128.79 (17) C6—C1—H10 120.2 (11)
N2—N3—C8 121.47 (15) C16—C15—F1 117.59 (17)
C7—C8—N3 120.55 (16) C16—C15—C14 124.80 (18)
C7—C8—C11 125.48 (17) F1—C15—C14 117.60 (17)
N3—C8—C11 113.65 (15) N4—C18—C19 103.35 (17)
C15—C16—C17 119.48 (19) N4—C18—H8A 111.4 (10)
C15—C16—H23 119.3 (12) C19—C18—H8A 111.9 (10)
C17—C16—H23 121.2 (12) N4—C18—H8B 109.5 (11)
N4—C17—C16 118.64 (16) C19—C18—H8B 112.8 (11)
N4—C17—C12 123.83 (16) H8A—C18—H8B 107.9 (15)
C16—C17—C12 117.52 (17) N1—C10—N3 110.9 (2)
C13—C12—C17 118.80 (17) N1—C10—H7 128.5 (12)
C13—C12—C11 116.20 (16) N3—C10—H7 120.6 (12)
C17—C12—C11 124.01 (16) N2—C9—N1 115.8 (2)
C9—N2—N3 101.55 (17) N2—C9—H6 120.1 (12)
C17—N4—C18 121.73 (16) N1—C9—H6 124.1 (12)
C17—N4—C21 124.29 (15) C13—C14—C15 115.96 (19)
C18—N4—C21 110.76 (15) C13—C14—H5 123.1 (12)
C14—C13—C12 123.04 (19) C15—C14—H5 120.9 (12)
C14—C13—H18 120.7 (11) C3—C4—C5 120.1 (2)
C12—C13—H18 116.2 (11) C3—C4—H4 120.3 (11)
C5—C6—C1 118.15 (17) C5—C4—H4 119.6 (11)
C5—C6—C7 117.39 (17) N4—C21—C20 104.23 (17)
C1—C6—C7 124.45 (18) N4—C21—H3A 108.6 (10)
O1—C11—C12 122.52 (16) C20—C21—H3A 113.9 (10)
O1—C11—C8 117.93 (16) N4—C21—H3B 109.3 (12)
C12—C11—C8 119.47 (16) C20—C21—H3B 112.6 (12)
C8—C7—C6 130.44 (18) H3A—C21—H3B 108.0 (15)
C8—C7—H15 114.9 (10) C21—C20—C19 103.03 (19)
C6—C7—H15 114.6 (10) C21—C20—H2A 110.8 (11)
C4—C3—C2 119.69 (19) C19—C20—H2A 112.1 (12)
C4—C3—H14 120.5 (12) C21—C20—H2B 110.3 (12)
C2—C3—H14 119.8 (12) C19—C20—H2B 114.9 (12)
C10—N1—C9 102.06 (18) H2A—C20—H2B 105.9 (17)
C4—C5—C6 121.24 (19) C20—C19—C18 102.69 (18)
C4—C5—H12 119.7 (11) C20—C19—H1A 112.8 (12)
C6—C5—H12 119.1 (11) C18—C19—H1A 110.9 (12)
C3—C2—C1 120.8 (2) C20—C19—H1B 110.2 (14)
C3—C2—H11 122.7 (11) C18—C19—H1B 110.3 (14)
C1—C2—H11 116.5 (12) H1A—C19—H1B 109.8 (18)
C2—C1—C6 120.0 (2)