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. 2012 May 5;68(Pt 6):o1663. doi: 10.1107/S1600536812019733
Bruker SMART 1K diffractometer 3498 independent reflections
Radiation source: fine-focus sealed tube 3132 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.031
φ and ω scans θmax = 28.4°, θmin = 2.3°
Absorption correction: multi-scan (SADABS; Bruker, 2001) h = −32→33
Tmin = 0.901, Tmax = 0.942 k = −12→12
12490 measured reflections l = −16→16