| Bruker SMART CCD area-detector diffractometer | 6399 independent reflections |
| Radiation source: fine-focus sealed tube | 4035 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.049 |
| phi and ω scans | θmax = 26.0°, θmin = 1.7° |
| Absorption correction: multi-scan (SADABS; Bruker, 1999) | h = −36→47 |
| Tmin = 0.982, Tmax = 0.993 | k = −15→15 |
| 10320 measured reflections | l = −12→11 |
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