| Bruker SMART CCD area-detector diffractometer | 2119 independent reflections |
| Radiation source: fine-focus sealed tube | 1828 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.023 |
| ω and φ scans | θmax = 25.0°, θmin = 2.2° |
| Absorption correction: multi-scan (SADABS; Bruker, 2001) | h = −15→15 |
| Tmin = 0.770, Tmax = 1.000 | k = −15→15 |
| 11097 measured reflections | l = −8→8 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.