| Siemens SMART 1K CCD diffractometer | 3295 independent reflections |
| Radiation source: normal-focus sealed tube | 2562 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.047 |
| ω scans | θmax = 26.8°, θmin = 2.0° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2000) | h = −13→13 |
| Tmin = 0.953, Tmax = 0.990 | k = −9→9 |
| 15768 measured reflections | l = −25→25 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.