| Enraf–Nonius CAD-4 diffractometer | Rint = 0.087 |
| Radiation source: fine-focus sealed tube | θmax = 25.4°, θmin = 1.9° |
| Graphite monochromator | h = 0→12 |
| ω/2θ scans | k = 0→20 |
| 4802 measured reflections | l = −17→16 |
| 4541 independent reflections | 3 standard reflections every 200 reflections |
| 2743 reflections with I > 2σ(I) | intensity decay: 1% |
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