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Deuterium incorporation in 9-MDTB and Biotin Derived From (2H-9-methyl)-DTB
| Number of Deuterium Atomsa | |||||
|---|---|---|---|---|---|
| Sample | 0 | 1 | 2 | 3 | 4 |
| DTB | 0.6% | 0.8% | 4% | 71% | 24% |
| MDTB | 9% | 7% | 56% | 21% | 6% |
| Biotin | 3% | 7% | 64% | 22% | 2% |
The percentage of each sample with the indicated number of deuterium atoms, after correcting for a natural abundance distribution of 13C (1.11 %) and 34S (4.2 %) at each position. The location of deuterium within each sample has not been determined.
