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. 2012 Apr 30;4(5):339–352. doi: 10.3390/toxins4050339

Table 7.

Recovery experiment with Certified Reference Material (NRC CRM-DSP-MUS-b). Samples were analysed with and without hydrolysis.

Without hydrolysis With hydrolysis
Matrix Spiked level (µg/kg) (n) Recovery RSDr Recovery RSDr
mussel 219 (4) 87% 14% 146% 12%
king scallop 180 (4) 91% 5.0% 163% 2.8%