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. Author manuscript; available in PMC: 2012 Oct 17.
Published in final edited form as: Inorg Chem. 2011 Aug 15;50(20):9794–9803. doi: 10.1021/ic200046k

Figure 5.

Figure 5

51V solid-state NMR spectra of the four vanadium(V)-o-dioxolene compounds of the series VVO-hshed (1a – 1c) (a–c) and [VO(acac)(TCCat)] (2) (d) obtained at a magnetic field of 9.4 T with MAS frequency of 17 kHz. 8192 scans were accumulated for each spectrum, and the pulse delay was 1.0 s. Experimental spectra are shown in black and best-fit simulated spectra are shown in red. The simulated spectra were obtained from SIMPSON using the NMR parameters listed in Table 1.